Structural characterization of a mechanically milled carbon nanotube ...
As a reference test, CNTs were first milled alone for times varying from 0 to 5 h in a high energy Spex 8000 this type of mill, a ballcontaining vial is shaken in a figure of 8 motion at a fixed speed of 1200 rpm and it is the impact of the balls against the sample and the end of the vial that induces milling and 7/16″ carbide balls and container with a 10:1 ballto ...